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Saxagliptin
Human APIstandards in stock
Route - KSMs and intermediates
- KSMBoc-3-Hydroxy adamantyl-D-Glycine (BHA)361442-00-4
- KSM(1S,3S,5S)-2-Azabicyclo[3.1.0]hexane-3- carboxamide Monomethanesulfonate (MPA)709031-45-8
- IntermediateN-[(1S)-2-[(1S,3S,5S)-3-cyano-2- azabicyclo[3.1.0]hex-2-yl]-1-(3- hydroxytricyclo[3.3.1.13,7]dec-1-yl)-2-oxoethyl]-Carbamic Acid 1,1-Dimethylethyl Ester (Boc-Saxagliptin)709031-43-6
Impurity and working standards - ready stock
| Structure | Standard | CAS | Availability | |
|---|---|---|---|---|
| API ((1S,3S,5S)-2-[(2S)-2- amino-2-(3 hydroxyadamantan-1- yl)acetyl]-2-azabicyclo[3. 1.0]hexane-3-carbonitrile hydrochloride) | 709031-78-7 | In stock | |
 | Boc Saxagiiptin | 709031-43-6 | In stock |
Characterised impurities
| Impurity | Chemical name | Pharmacopoeia |
|---|---|---|
| MPA TMEDA | (1S,3S,5S)-2- Azabiocyclo[3.1.0]he xane-3-carboxamide monomethanesulfon ate N,N,N,N- Tetramethylethylene diamine (TMEDA) | IHT IHT |
| Ethyl Nicotinate BHA | Ethyl pyridine-3- carboxylate BOC-3-Hydroxy-1- adamantyl-D- Glycine | IHT IHT |
| HOBT.H2O saxagliptin HCl Deboc- BHP impurity (S)-2- Amino-2- ((1r,3R,5R,7 S)-3- hydroxyad amantan- 1-yl)acetic | Hydroxybenzotriazol monohydrae saxagliptin HCl 3-Descarbonitrile-3- acetamide Saxegliptin (S)-2-Amino-2- ((1r,3R,5R,7S)-3- hydroxyadamantan- 1-yl)acetic acid | IHT IHT IHT IHT |
| acid (S)-2- (Adamanta n-1-yl)-2- (((R)-2- hydroxy-1- phenyleth yl)amino)a cetic acid (Adamanta ne hydroxy acetic acid) (R)-BHA of saxagliptin | (S)-2-(Adamantan-1- yl)-2-(((R)-2-hydroxy- phenylethyl)amino)a cetic acid (Adamantane hydroxy acetic acid) BOC-3-hydroxy-1- adamantyl-L-glycin; (R)-2-((tert- butoxycarbonyl)ami no)-2- ((1R.3S.5R.7S)-3- hydroxyadamantan- 1-yl)acetic acid | IHT IHT |
| Deboc- BHP impurity DIPEA | 3-Descarbonitrile-3- acetamide Saxegliptin N,N- Diisopropylethylami | IHT IHT |
| Ethyl acetoaceta te DPS | Ethyl acetoacetate | IHT IHT |
| EDC.HCl | hydrochloride; (N- ethyl-N'-(3- dimethylaminopropy l)carbodiimide hydrochloride | IHT |
| TFAA | Trifluoro acetic anhydride | IHT |
| Impurity "A" | (Dimethylamino)ethy l]-2-[[3-[2- (dimethylamino)ethy l]-1H-indol-5- yl]methyl]-1H-indol- 5-yl]-N-methyl methanesulfonamid | USP/EP |
| Impurity “C” | (dimethylamino)ethy (hydroxymethyl)-1H- indol-5-yl]- Nmethylmethanesul phonamide, | EP/USP |
| Impurity “D” | N,N-dimethyl-2-[5- [(methylsulphamoyl) methyl]-1H-indol-3- yl]ethanamine N- | EP |
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